%0 Journal Article %T Synthesis and Characterization of CuIn<sub>2n+1</sub> S<sub>3n+2</sub> (with n = 0, 1, 2, 3 and 5) Powders %A Naoufel Khemiri %A Dhafer Abdelkader %A Bilel Khalfallah %A Mounir Kanzari %J Open Journal of Synthesis Theory and Applications %P 33-37 %@ 2168-1252 %D 2013 %I Scientific Research Publishing %R 10.4236/ojsta.2013.21003 %X

CuIn2n+1 S3n+2 crystals were synthesized by horizontal Bridgman method using high purity copper, indium, sulfur elements. The phases and crystallographic structure of the CuIn2n+1S3n+2 crystals were analyzed by X-ray diffraction (XRD) and the composition of the material powders was determined using the energy dispersive X-ray analysis (EDX). Measurement data revealed that CuIn2n+1S3n+2 materials have not the same structure. In fact, CuInS2 and CuIn3S5 crystallize in the chalcopyrite structure whereas CuIn5S8, CuIn7S11 and CuIn11S17 crystallize in the cubic spinel structure.

 

%K CuIn< %K sub> %K 2n+1< %K /sub> %K S< %K sub> %K 3n+2< %K /sub> %K Synthesis %K Structural Properties %U http://www.scirp.org/journal/PaperInformation.aspx?PaperID=27197