%0 Journal Article
%T Synthesis and crystal structure of 2-methoxy-4,6-bis(4-nitrophenoxy)-1,3,5-triazine
%A Huang Yuanyuan
%A Bai Fang
%A Gao Guowei
%A Men Jian
%J European Journal of Chemistry
%D 2012
%I 
%R 10.5155/eurjchem.3.1.17-20.534
%X The novel compound, 2-methoxy-4,6-bis(4-nitrophenoxy)-1,3,5-triazine has been synthesized starting from 2,4,6-trichloro-1,3,5-triazine and characterized by 1H NMR, 13C NMR, IR, mass spectroscopy and elemental analysis. The single crystal of the title compound was obtained and subjected to X-ray diffraction analysis. The single crystal data illustrates that it belongs to the monoclinic system, space group C2/c with a = 13.818(3)  , b = 7.8964(16)  , c = 30.718(6)  , ¦Â = 96.52(3) o, V = 3330.0(12)  3, Z = 8, Dc = 1.537 g/cm3, C16H11N5O7, Mr = 385.30, ¦Ì (MoK¦Á) = 0.124 mm 1, F(000) = 1584, the final R = 0.0489 and wR = 0.1821 for 2491 observed reflections with I>2¦Ò(I).
%K Synthesis
%K Bis-maleimides
%K ¦Ð-¦Ð Interactions
%K Crystal structure
%K 2
%K 4
%K 6-Trichloro-1
%K 3
%K 5-triazine
%K 2-Methoxy-4
%K 6-bis(4-nitrophenoxy)-1
%K 3
%K 5-triazine
%U http://www.eurjchem.com/index.php/eurjchem/article/view/534