%0 Journal Article
%T 均苯三乙酮的合成研究<br>Study on Synthesis of 1,3,5-Triacetylbenzene
%A 张精安
%A 邹训重
%A 刘亚杰
%A 张莉杰
%A 欧意桃
%A 程燕芳
%J Studies in Synthetic Chemistry
%P 58-63
%@ 2332-7960
%D 2015
%I Hans Publishing
%R 10.12677/SSC.2015.33009
%X <div style=\"text-align:justify;\">
	<span style=\"line-height:1.5;\">目的：合成均苯三乙酮。方法：利用甲酸乙酯、丙酮和乙醇钠反应生成不饱和醇钠，然后用弱酸酸化生成均苯三乙酮。结果：成功合成出均苯三乙酮，并通过TLC监测、测定其熔点及质谱和核磁共振氢谱确定其结构。结论：此合成均苯三乙酮的方法操作简单，原料价廉易得，可用于工业上合成较大量的均苯三乙酮。<br />
Objective: 1,3,5-Triacetylbenzene was synthesized. Methods: 1,3,5-Triacetylbenzene was prepared by ethyl formate and acetone reaction with sodium ethoxide and then the producing unsaturated sodium ethoxide solution was acidified with weak acid. Results: 1,3,5-Triacetylbenzene was synthesized and confirmed by TLC, melting point, 13C-NMR and 1H-NMR. Conclusion: The operating method of the synthesis of 1,3,5-triacetylbenzene was simple, cheap and easily available for the raw materials, so it could be used for the industrial synthesis of relatively large quantities.</span><span style=\"line-height:1.5;\"></span> 
</div>
%K 均苯三乙酮，甲酸乙酯，丙酮，合成<br>1.3.5-Triacetylbenzene
%K Ethyl Formate
%K Acetone
%K Synthesis
%U http://www.hanspub.org/journal/PaperInformation.aspx?PaperID=16011