%0 Journal Article
%T PREPARATION AND CHARACTERIZATION OF BONDED-PHASES OF CALIXARENE-SULFONYL-CARBOXAMIDES IN PARTIAL-CONE CONFORMATION FOR DETERMINATION OF SALBUTAMOL IN LIVESTOCK BY NANO-MEDIATED BONDED-PHASES: NANO-BASKETS OF CALIXARENE IN PARTIAL-CONE CONFORMATION
%A MOKHTARI
%A BAHRAM
%A POURABDOLLAH
%A KOBRA
%J Journal of the Chilean Chemical Society
%D 2012
%I Scientific Electronic Library Online
%R 10.4067/S0717-97072012000200020
%X a new sensitive method for determination of salbutamol, as a nutrient repartitioning agent, in livestock is presented to protect the consumers. eight nano-baskets of p-tert-calix[4]arene bearing di-[n-(x)sulfonyl carboxamide] and di-(1-propoxy) in partial-cone conformation were synthesized and were used to prepare bended phases of hplc-uv. the new synthesized bonded-phases were characterized and optimized, the bonding interactions of solute and stationary phases were examined and the main interactions were reported. the results revealed that for the best bonded-phase, the lod and loq were 0.02 and 0.06 ¦Ìg/ml, respectively.
%K bonded-phase
%K partial-cone conformation
%K calixarene
%K salbutamol
%K nanobasket.
%U http://www.scielo.cl/scielo.php?script=sci_abstract&pid=S0717-97072012000200020&lng=en&nrm=iso&tlng=en