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Preparation Characterization and Thermal Behaviour of Carbopol-TiO2 Nanocomposites

DOI: 10.4236/ojopm.2014.43008, PP. 55-64

Keywords: Carbopol, TiO2-Fellers, Nanocomposite, Thermal Proprieties, FT-IR Spectroscopy

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Abstract:

Composites consisting of carbopol (CP) and ceramic titanium dioxide nanoparticles, TiO2 have been investigated. The CP-TiO2, organic-inorganic hybrid composites have been prepared in DMF by heating the mixture with a constant rate of 1C/min, up to 30C, 45C, 60C, 80C, 100C and 120C. Proprieties such as absorption, structure and external aspect of the obtained materials were investigated by Uv-vis, FTIR, DRX and SEM analyses. The X-ray diffraction patterns confirmed that the TiO2 nanoparticles maintained their original tetragonal anatase-type crystalline structure in the composites. The chemical structure of the obtained materials was determined by ATR-FTIR spectroscopy. The influence of TiO2 nanoparticles on the thermal proprieties of carbopol matrix was investigated using thermo-gravimetric analysis and differential scanning calorimetry. The glass transition temperature

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