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Synthesis of the Palladium Catalyst with the Supercritical СO2-Impregnation Method Realized in the Static Mode

DOI: 10.4236/ijamsc.2014.24010, PP. 113-122

Keywords: Supercritical Carbon Dioxide, Aluminum Oxide, Impregnation, Palladium Catalyst, Activity

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Abstract:

Results of research of supercritical fluid CO2-impregnation process (the static mode) within a problem of synthesis of the palladium catalyst are given. The kinetics of process is characterized in the pressure range from 15.0 to 35.0 MPa on temperatures 308.15?K, 313.15?K, 318.15?K, 323.15?K, 328.15?K and 333.15?K. Results of surface assessment and activity measurements of the catalyst samples synthesized by supercritical СO2-impregnation of aluminum oxide suggest competitiveness of the discussed approach in comparison to traditional methods.

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