全部 标题 作者
关键词 摘要

OALib Journal期刊
ISSN: 2333-9721
费用:99美元

查看量下载量

相关文章

更多...
化工学报  2015 

分子蒸馏、薄膜蒸发与精馏耦合技术分离肉桂油组分

DOI: 10.11949/j.issn.0438-1157.20150895, PP. 3542-3548

Keywords: 肉桂油,蒸馏,预测,优化,分离

Full-Text   Cite this paper   Add to My Lib

Abstract:

本文采用分子蒸馏、薄膜蒸发与精馏耦合技术对肉桂油主要成分的分离进行研究。系统的温度、压力和回流比对5种组分的得率和纯度的影响分别进行了研究,实验结果表明这种技术成功地用于分离肉桂油。为了进一步理解分离因素相互之间对分离效果的影响,本文选择肉桂醛为模型化合物,采用中心响应面法对肉桂醛分离的影响因素进行研究。实验结果表明:温度95℃,压力50Pa时,肉桂醛的得率和纯度最高。实验验证的数值与响应面法模拟的数值一致,表明响应面法可以用于指导肉桂油的生产。

References

[1]  Ruan Haiyan(阮海燕). Application of cinnamaldehyde in essence and flavor daily chemical and food additive industries [J]. Fine and Specialty Chemicals(精细与专用化学品), 2005, 13(3): 9-10.
[2]  Li Yanliang, Fang Zhixiang, You Jing. Application of Box-Behnken experimental design to optimize the extraction of insecticidal Cry1Ac from soil [J]. J. Agric. Food. Chem., 2013, 61(2): 1464-1470.
[3]  Akitha Devi M K, Giridhar P. Isoflavone augmentation in soybean cell cultures is optimized using response surface methodology [J]. J. Agric. Food Chem., 2014, 62(14): 3143-3149.
[4]  Wang Shiyi(王世仪), Zhang Li(张丽), Wang Bing(王冰), Li Wenyan(李文颜). Bacteriological study of Chinese herbs cinnamicaldehyde on disinfection of infection root canal [J]. Chinese Journal of Microecology(中国微生态学杂志), 2000, 12(6): 369-373.
[5]  Yang Xia(杨霞), Huang Ping(黄萍), Xiao Xiaorong(肖晓蓉), Li Conghua(李从华). Antibacterial activities of Chinese medicine cinnamicaldehyde against main periodontal pathogen [J]. Chongqing Medicine(重庆医学), 2009, 38(1): 75-76.
[6]  Bi Wen(毕文). Research of antimicrobial substance in cinnamon oil [J]. Gansu Science and Technology(甘肃科技), 2012, 28(9): 145-146.
[7]  Tang Yufang(唐裕芳), Zhang Miaoling(张妙玲), Huang Baifei(黄白飞). The extraction and Anti-microbial activity of cinnamon oil [J]. Nat. Prod. Res. Dev.(天然产物研究与开发), 2006, 18(3): 432-433.
[8]  Yu H S, Lee S Y, Jang C G. Involvement of 5- HTlA and GABAA receptors in the anxiolytic-like effects of Cinnamomum cassia inmice [J]. Pharmacol. Biochem. Behav., 2007, 87(1): 164-170.
[9]  Yen T B, Chang S T. Synergistic effects of cinnamaldehyde in combination with eugenol against wood decay fungi [J]. Bioresour. Technol., 2008, 99(1): 232-236.
[10]  Wang R, Wang R J, Yang B. Extraction of essential oils from five cinnamon leaves and identification of their volatile compound compositions [J]. Innov. Food. Sci. Emerg., 2009, 10(2): 289-292.
[11]  Yang C H, Li R X, Chuang L Y. Antioxidant activity of various parts of Cinnamomum cassia extracted with different extraction methods [J]. Molecules, 2012, 17(6): 7294-7304.
[12]  Yu Jianliang(喻健良), Qu Zhiyong(翟志勇). Development of molecular distillation technique [J]. Chemical Engineering(化学工程), 2001, 29(5): 70-74.
[13]  Zhu Shunqin(祝顺琴), Tan Feng(谈锋). Application of molecular distillation technique in separation of natural products [J]. Fine Chemicals (精细化工), 2004, 21(1): 46-50.
[14]  Burch C R. Some experiments on vacuum distillation [J]. Proceedings of the Royal Society of London: Series A, 1929, 123(791): 271-284.
[15]  Wang Junwu(王军武), Xu Songlin(许松林), Xu Shimin(徐世民), Gan Aihua(干爱华). Application status of molecular distillation technology [J]. Chemical Industry and Engineering Progress(化工进展), 2002, 21(7): 499-501.
[16]  Wang Mingyan(王明艳), Zhang Xiaojie(张小杰), Wang Tao(王涛), Ma Weixing(马卫兴), Xu Xingyou(许兴友). Response surface methodology for optimizing extraction of polysaccharides from Toona sinensis (A. Juss.) Roem leaves[J]. Food Sci.(食品科学), 2010, 31(4): 106-110.
[17]  Khayet M, Cojocaru C, Garcia-Payo C. Application of response surface methodology and experimental design in direct contact membrane distillation [J]. Ind. Eng. Chem. Res., 2007, 46(17): 5673-5685.
[18]  Zhang D, Li S, Xiong Q, et al. Extraction, characterization and biological activities of polysaccharides from Amomum villosum[J]. Carbohydr. Polym., 2013, 95(1): 114-122.
[19]  Hollebeeck S, Borlon F, Schneider Y, et al. Development of a standardized human in vitro digestion protocol based on macronutrient digestion using reponse surface methodology [J]. Food Chem., 2013, 138(2): 1936-1944.
[20]  Lu C H, Engelmann N, Lila M A, Erdman J W. Optimization of lycopene extraction from tomato cell suspension culture by response surface methodology [J]. J. Agric. Food Chem., 2008, 56: 7710-7714.
[21]  Sujoy B, Chandan D. Role of binder and preparation pressure in tubular ceramic membrane processing: design and optimization study using response surface methodology [J]. Ind. Eng. Chem. Res., 2014, 53(31): 12319-12329.

Full-Text

comments powered by Disqus

Contact Us

service@oalib.com

QQ:3279437679

WhatsApp +8615387084133