54 Wang Z L,Xu D,Huang Y,et al.Facile,mild and fast thermal-decomposition reduction of graphene oxide in air and its application in high-performance lithium batteries.Chem Commun,2012,48:976-978
[2]
55 Wang Z J,Zhou X Z,Zhang J,et al.Direct electrochemical reduction of single-layer graphene oxide and subsequent functionalization with glucose oxidase.J Phys Chem C,2009,113:14071-14075
[3]
56 Zhou X Z,Huang X,Qi X Y,et al.In situ synthesis of metal nanoparticles on single-layer graphene oxide and reduced graphene oxide surfaces.J Phys Chem C,2009,113:10842-10846
[4]
57 Donner S,Li H W,Yeung E S,et al.Fabrication of optically transparent carbon electrodes by the pyrolysis of pho toresist films:Ap- proach to single-molecule spectroelectrochemistry.Anal Chem,2006,78:2816-2822
[5]
58 Qi X Y,Pu K Y,Zhou X Z,et al.Conjugated-polyelectrolyte-functionalized reduced graphene oxide with excellent solubility and stability in polar solvents.Small,2010,6:663-669
[6]
59 Williams G,Seger B,Kamat P V.TiO2-graphene nanocomposites.UV-assisted photocatalytic reduction of graphene oxide.ACS Nano,2008,2:1487-1491
[7]
60 Gao J,Liu F,Liu Y L,et al.Environment-friendly method to produce graphene that employs vitamin c and amino acid.Chem Mater,2010,22:2213-2218
[8]
61 Hernandez Y,Nicolosi V,Lotya M,et al.High-yield production of graphene by liquid-phase exfoliation of graphite.Nat Nanotechnol,2008,3:563-568
[9]
62 Khan U,Porwal H,O'Neill A,et al.Solvent-exfoliated graphene at extremely high concentration.Langmuir,2011,27:9077-9082
[10]
75 An X,Simmons T,Shah R,et al.Stable aqueous dispersions of noncovalently functionalized graphene from graphite and their m ultifunc- tional high-performance applications.Nano Lett,2010,10:4295-4301
[11]
76 Veca L M,Lu F,Meziani M J,et al.Polymer functionalization and solubilization of carbon nanosheets.Chem Commun,2009,10:2565-2567
[12]
77 Xu Y X,Bai H,Lu G W,et al.Flexible graphene films via the filtration of water-soluble noncovalent functionalized graphene sheets.J Am Chem Soc,2008,130:5856-5857
[13]
78 Hao R,Qian W,Zhang L H,et al.Aqueous dispersions of TCNQ-anion-stabilized graphene sheets.Chem Commun,2008,48:6576-6578
[14]
79 Li X L,Wang X R,Zhang L,et al.Chemically derived,ultrasmooth graphene nanoribbon semiconductors.Science,2008,319:1229-1232
[15]
80 Li X L,Zhang G Y,Bai X D,et al.Highly conducting graphene sheets and langmuir-blodgett films.Nat Nanotechnol.,2008,3:538-542
[16]
81 Qi X,Pu K Y,Li H,et al.Amphiphilic graphene composites.Angew Chem Int Ed,2010,49:9426-9429
[17]
82 Eckert C A,Knutson B L,Debenedetti P G.Supercritical fluids as solvents for chemical and materials processing.Nature,199 6,383:313-318
[18]
83 Chaudhary A,Beckman E J,Russell A J.Rational control of polymer molecular weight and dispersity during enzyme-catalyzed polyester synthesis in supercritical fluids.J Am Chem Soc,1995,117:3728-3733
[19]
84 Serhatkulu G K,Dilek C,Gulari E.Supercritical CO2 intercalation of layered silicates.J Supercrit Fluid,2006,39:264-270
[20]
85 Johnston K P,Shah P S.Making nanoscale materials with supercritical fluids.Science,2004,303:482-483
[21]
86 Pu N W,Wang C A,Sung Y,et al.Production of few-layer graphene by supercritical CO2 exfoliation of graphite.Mater Lett,2009,63:1987-1989
[22]
87 Horsch S,Serhatkulu G,Gulari E,et al.Supercritical CO2 dispersion of nano-clays and clay/polymer nanocomposites.Polymer,2006,47:7485-7496
[23]
88 Li J,Xu Q,Peng Q,et al.Supercritical CO2-assisted synthesis of polystyrene/clay nanocomposites via in situ intercalative polymerization. J Appl Poly Sci,2006,100:671-676
[24]
89 Zheng X L,Xu Q,Li J B,et al.High-throughput,direct exfoliation of graphite to graphene via a cooperation of supercritical CO 2 and pyrene-polymers.RSC Adv,2012,2:10632-10638
[25]
90 Rangappa D,Sone K,Wang M,et al.Rapid and direct conversion of graphite crystals into high-yielding,good-quality graphene by su- percritical fluid exfoliation.Chem Eur J,2010:16:6488-6494
[26]
91 Liu C,Hu G,Gao H.Preparation of few-layer and single-layer graphene by exfoliation of expandable graphite in supercritical N,N-dimethylformamide.J Supercrit Fluid,2012,63:99-104
[27]
92 Jang J H,Rangappa D,Kwon Y U,et al.Direct preparation of 1-PSA modified graphene nanosheets by supercritical fluidic exfoliation and its electrochemical properties.J Mater Chem,2011,21:3462-3466
[28]
93 Li L H,Zheng X L,Wang J J,et al.Solvent-exfoliated and functionalized graphene with assistance of supercritical carbon dioxide.ACS Sust Chem Eng,2013,1:144-151
[29]
94 Li L H,Zhang J N,Liu Y Q,et al.Facile fabrication of Pt nanoparticles on 1-pyrenamine functionalized graphene nanosheets for metha- nol electrooxidation.ACS Sust Chem Eng,2013,1:527-533
[30]
95 Petrov P,Stassin F,Pagnoulle C,et al.Noncovalent functionalization of multi-walled carbon nanotubes by pyrene containing polymers. Chem Commun,2003,(23):2904-2905
[31]
96 Etika K C,Jochum F D,Theato P,et al.Temperature controlled dispersion of carbon nanotubes in water with pyrene-functionalized poly(N-cyclopropylacrylamide).J Am Chem Soc,2009,131:13598-13599
[32]
97 Liu J,Bibari O,Mailley P,et al.Stable non-covalent functionalisation of multi-walled carbon nanotubes by pyrene-polyethylene glycol throughπ-πstacking.New J Chem,2009,33:1017-1024
[33]
98 Yan Y,Cui J,P?tschke P,et al.Dispersion of pristine single-walled carbon nanotubes using pyrene-capped polystyrene and its application for preparation of polystyrene matrix composites.Carbon,2010,48:2603-2612
[34]
99 Knights S D,Colbow K M,St-Pierre J,et al.Aging mechanisms and lifetime of PEFC and DMFC.J Power Sources,2004,127:127-134
[35]
100 Kundu P,Nethravathi C,Deshpande P A,et al.Ultrafast microwave-assisted route to surfactant-free ultrafine Pt nanoparticles on gra- phene:Synergistic co-reduction mechanism and high catalytic activity.Chem Mater,2011,23:2772-2780
[36]
101 Wang S,Wang X,Jiang S P.PtRu nanoparticles supported on 1-aminopyrene-functionalized multiwalled carbon nanotubes and their electrocatalytic activity for methanol oxidation.Langmuir,2008,24:10505-10512
[37]
102 Zhang W,Chen J,Swiegers G F,et al.Microwave-assisted synthesis of Pt/CNT nanocomposite electrocatalysts for PEM fuel cells.Na- noscale,2010,2:282-286
[38]
103 Sharma S,Ganguly A,Papakonstantinou P,et al.Rapid microwave synthesis of CO tolerant reduced graphene oxide-supported platinum electrocatalysts for oxidation of methanol.J Phys Chem C,2010,114:19459-19466
[39]
104 Huang H J,Chen H Q,Sun D P,et al.Graphene nanoplate-Pt composite as a high performance electrocatalyst for direct methanol fuel cells.J Power Sources,2012,204:46-52
[40]
105 Khosravi M,Amini M K.Flame synthesis of carbon nanofibers on carbon paper:Physicochemical characterization and application as catalyst support for methanol oxidation.Carbon,2010,48:3131-3138
[41]
106 Xin Y C,Liu J G,Jie X,et al.Preparation and electrochemical characterization of nitrogen doped graphene by microwave as supporting materials for fuel cell catalysts.Electro Acta,2012,60:354-358 ?
[42]
52 Chen W, Yan L, Bangal P R.Preparation of graphene by the rapid and mild thermal reduction of graphene oxide induced by microwaves.Carbon, 2010, 48:1146-1152
[43]
53 Schniepp H C, Li J L, McAllister M J, et al.Functionalized single graphene sheets derived from splitting graphite oxide.J Phys Chem B, 2006, 110:8535-8539
[44]
54 Wang Z L, Xu D, Huang Y, et al.Facile, mild and fast thermal-decomposition reduction of graphene oxide in air and its application in high-performance lithium batteries.Chem Commun, 2012, 48:976-978
[45]
55 Wang Z J, Zhou X Z, Zhang J, et al.Direct electrochemical reduction of single-layer graphene oxide and subsequent functionalization with glucose oxidase.J Phys Chem C, 2009, 113:14071-14075
[46]
56 Zhou X Z, Huang X, Qi X Y, et al.In situ synthesis of metal nanoparticles on single-layer graphene oxide and reduced graphene oxide surfaces.J Phys Chem C, 2009, 113:10842-10846
[47]
57 Donner S, Li H W, Yeung E S, et al.Fabrication of optically transparent carbon electrodes by the pyrolysis of photoresist films: Approach to single-molecule spectroelectrochemistry.Anal Chem, 2006, 78:2816-2822
[48]
58 Qi X Y, Pu K Y, Zhou X Z, et al.Conjugated-polyelectrolyte-functionalized reduced graphene oxide with excellent solubility and stability in polar solvents.Small, 2010, 6:663-669
[49]
59 Williams G, Seger B, Kamat P V.TiO2-graphene nanocomposites.UV-assisted photocatalytic reduction of graphene oxide.ACS Nano, 2008, 2:1487-1491
[50]
60 Gao J, Liu F, Liu Y L, et al.Environment-friendly method to produce graphene that employs vitamin c and amino acid.Chem Mater, 2010, 22:2213-2218
[51]
61 Hernandez Y, Nicolosi V, Lotya M, et al.High-yield production of graphene by liquid-phase exfoliation of graphite.Nat Nanotechnol, 2008, 3:563-568
[52]
62 Khan U, Porwal H, O’Neill A, et al.Solvent-exfoliated graphene at extremely high concentration.Langmuir, 2011, 27:9077-9082
[53]
63 Lotya M, Hernandez Y, King P J, et al.Liquid phase production of graphene by exfoliation of graphite in surfactant/water solutions.J Am Chem Soc, 2009, 131:3611-3620
[54]
64 O’Neill A, Khan U, Nirmalraj P N, et al.Graphene dispersion and exfoliation in low boiling point solvents.J Phys Chem C, 2011, 115:5422-5428
[55]
65 Hernandez Y, Lotya M, Rickard D, et al.Measurement of multicomponent solubility parameters for graphene facilitates solvent discovery.Langmuir, 2010, 26:3208-3213
[56]
66 Khan U, O’Neill A, Lotya M, et al.High-concentration solvent exfoliation of graphene.Small, 2010, 6:864-871
[57]
67 Khan U, O’Neill A, Porwal H, et al.Size selection of dispersed, exfoliated graphene flakes by controlled centrifugation.Carbon, 2012, 50:470-475
[58]
68 Keeley G P, O’Neill A, Holzinger M, et al.DMF-exfoliated graphene for electrochemical nadh detection.Phys Chem Chem Phys, 2011, 13:7747-7750
[59]
69 Hamilton C E, Lomeda J R, Sun Z, et al.High-yield organic dispersions of unfunctionalized graphene.Nano Lett, 2009, 9:3460-3462
[60]
70 Coleman J N.Liquid-phase exfoliation of nanotubes and graphene.Adv Func Mater, 2009, 19:3680-3695
[61]
71 Hummers W S, Offeman R E.Preparation of graphitic oxide.J Am Chem Soc, 1958, 80:1339-1339
[62]
72 Brodie B C.On the atomic weight of graphite.Philos Trans R Soc london, 1859, 149:249-259
[63]
73 Staudenmaier L.Verfahren zur darstellung der graphitsaure.Ber Deut Chem Ges, 1898, 31:1481-1499
[64]
74 Dhakate S R, Chauhan N, Sharma S, et al.An approach to produce single and double layer graphene from re-exfoliation of expanded graphite.Carbon, 2011, 49:1946-1954
[65]
75 An X, Simmons T, Shah R, et al.Stable aqueous dispersions of noncovalently functionalized graphene from graphite and their multifunctional high-performance applications.Nano Lett, 2010, 10:4295-4301
[66]
76 Veca L M, Lu F, Meziani M J, et al.Polymer functionalization and solubilization of carbon nanosheets.Chem Commun, 2009, 10:2565-2567
[67]
77 Xu Y X, Bai H, Lu G W, et al.Flexible graphene films via the filtration of water-soluble noncovalent functionalized graphene sheets.J Am Chem Soc, 2008, 130:5856-5857
[68]
78 Hao R, Qian W, Zhang L H, et al.Aqueous dispersions of TCNQ-anion-stabilized graphene sheets.Chem Commun, 2008, 48:6576-6578
[69]
79 Li X L, Wang X R, Zhang L, et al.Chemically derived, ultrasmooth graphene nanoribbon semiconductors.Science, 2008, 319:1229-1232
[70]
80 Li X L, Zhang G Y, Bai X D, et al.Highly conducting graphene sheets and langmuir-blodgett films.Nat Nanotechnol, 2008, 3:538-542
[71]
81 Qi X, Pu K Y, Li H, et al.Amphiphilic graphene composites.Angew Chem Int Ed, 2010, 49:9426-9429
[72]
82 Eckert C A, Knutson B L, Debenedetti P G.Supercritical fluids as solvents for chemical and materials processing.Nature, 1996, 383:313-318
[73]
83 Chaudhary A, Beckman E J, Russell A J.Rational control of polymer molecular weight and dispersity during enzyme-catalyzed polyester synthesis in supercritical fluids.J Am Chem Soc, 1995, 117:3728-3733
[74]
84 Serhatkulu G K, Dilek C, Gulari E.Supercritical CO2 intercalation of layered silicates.J Supercrit Fluid, 2006, 39:264-270
[75]
85 Johnston K P, Shah P S.Making nanoscale materials with supercritical fluids.Science, 2004, 303:482-483
[76]
86 Pu N W, Wang C A, Sung Y, et al.Production of few-layer graphene by supercritical CO2 exfoliation of graphite.Mater Lett, 2009, 63:1987-1989
[77]
87 Horsch S, Serhatkulu G, Gulari E, et al.Supercritical CO2 dispersion of nano-clays and clay/polymer nanocomposites.Polymer, 2006, 47:7485-7496
[78]
88 Li J, Xu Q, Peng Q, et al.Supercritical CO2-assisted synthesis of polystyrene/clay nanocomposites via in situ intercalative polymerization.J Appl Poly Sci, 2006, 100:671-676
[79]
89 Zheng X L, Xu Q, Li J B, et al.High-throughput, direct exfoliation of graphite to graphene via a cooperation of supercritical CO2 and pyrene-polymers.RSC Adv, 2012, 2:10632-10638
[80]
90 Rangappa D, Sone K, Wang M, et al.Rapid and direct conversion of graphite crystals into high-yielding, good-quality graphene by supercritical fluid exfoliation.Chem Eur J, 2010:16:6488-6494
[81]
91 Liu C, Hu G, Gao H.Preparation of few-layer and single-layer graphene by exfoliation of expandable graphite in supercritical N,N-dimethylformamide.J Supercrit Fluid, 2012, 63:99-104
[82]
92 Jang J H, Rangappa D, Kwon Y U, et al.Direct preparation of 1-PSA modified graphene nanosheets by supercritical fluidic exfoliation and its electrochemical properties.J Mater Chem, 2011, 21:3462-3466
[83]
93 Li L H, Zheng X L, Wang J J, et al.Solvent-exfoliated and functionalized graphene with assistance of supercritical carbon dioxide.ACS Sust Chem Eng, 2013, 1:144-151
[84]
94 Li L H, Zhang J N, Liu Y Q, et al.Facile fabrication of Pt nanoparticles on 1-pyrenamine functionalized graphene nanosheets for methanol electrooxidation.ACS Sust Chem Eng, 2013, 1:527-533
[85]
95 Petrov P, Stassin F, Pagnoulle C, et al.Noncovalent functionalization of multi-walled carbon nanotubes by pyrene containing polymers.Chem Commun, 2003, (23):2904-2905
[86]
96 Etika K C, Jochum F D, Theato P, et al.Temperature controlled dispersion of carbon nanotubes in water with pyrene-functionalized poly(N-cyclopropylacrylamide).J Am Chem Soc, 2009, 131:13598-13599
[87]
97 Liu J, Bibari O, Mailley P, et al.Stable non-covalent functionalisation of multi-walled carbon nanotubes by pyrene-polyethylene glycol through π-π stacking.New J Chem, 2009, 33:1017-1024
[88]
98 Yan Y, Cui J, P?tschke P, et al.Dispersion of pristine single-walled carbon nanotubes using pyrene-capped polystyrene and its application for preparation of polystyrene matrix composites.Carbon, 2010, 48:2603-2612
[89]
99 Knights S D, Colbow K M, St-Pierre J, et al.Aging mechanisms and lifetime of PEFC and DMFC.J Power Sources, 2004, 127:127-134
[90]
100 Kundu P, Nethravathi C, Deshpande P A, et al.Ultrafast microwave-assisted route to surfactant-free ultrafine Pt nanoparticles on graphene:Synergistic co-reduction mechanism and high catalytic activity.Chem Mater, 2011, 23:2772-2780
[91]
101 Wang S, Wang X, Jiang S P.PtRu nanoparticles supported on 1-aminopyrene-functionalized multiwalled carbon nanotubes and their electrocatalytic activity for methanol oxidation.Langmuir, 2008, 24:10505-10512
[92]
102 Zhang W, Chen J, Swiegers G F, et al.Microwave-assisted synthesis of Pt/CNT nanocomposite electrocatalysts for PEM fuel cells.Nanoscale, 2010, 2:282-286
[93]
103 Sharma S, Ganguly A, Papakonstantinou P, et al.Rapid microwave synthesis of CO tolerant reduced graphene oxide-supported platinum electrocatalysts for oxidation of methanol.J Phys Chem C, 2010, 114:19459-19466
[94]
104 Huang H J, Chen H Q, Sun D P, et al.Graphene nanoplate-Pt composite as a high performance electrocatalyst for direct methanol fuel cells.J Power Sources, 2012, 204:46-52
[95]
105 Khosravi M, Amini M K.Flame synthesis of carbon nanofibers on carbon paper:Physicochemical characterization and application as catalyst support for methanol oxidation.Carbon, 2010, 48:3131-3138
[96]
106 Xin Y C, Liu J G, Jie X, et al.Preparation and electrochemical characterization of nitrogen doped graphene by microwave as supporting materials for fuel cell catalysts.Electro Acta, 2012, 60:354-3587 Park S,Ruoff R S.Chemical methods for the production of graphenes.Nat Nanotechnol,2009,4:217-224
[97]
8 Stoller M D,Park S,Zhu Y,et al.Graphene-based ultracapacitors.Nano Lett,2008,8:3498-3502
[98]
9 Nair R R,Blake P,Grigorenko A N,et al.Fine structure constant defines visual transparency of graphene.Science,2008,320:1308
[99]
10 Novoselov K S,Geim A K,Morozov S V,et al.Two-dimensional gas of massless dirac fermions in graphene.Nature,2005,438:197-200
[100]
11 Kim H,Abdala A A,Macosko C W.Graphene/polymer nanocomposites.Macromolecules,2010,43:6515-6530
[101]
12 Liu Y C,Dong X C,Chen P.Biological and chemical sensors based on graphene materials.Chem Soc Rev,2012,41:2283-2307
[102]
13 Bai H,Li C,Shi G Q.Functional composite materials based on chemically converted graphene.Adv Mater,2011,23:1089-1115
[103]
14 Huang X,Zeng Z Y,Fan Z X,et al.Graphene-based electrodes.Adv Mater,2012,24:5979-6004
17 Sutter P W,Flege J I,Sutter E A.Epitaxial graphene on ruthenium.Nat Mater,2008,7:406-411
[107]
18 Reina A,Jia X,Ho J,et al.Large area,few-layer graphene films on arbitrary substrates by chemical vapor deposition.Nano Lett,2008,9:30-35
[108]
19 Chae S J,Güne?2015-6-19F,Kim K K,et al.Synthesis of large-area graphene layers on poly-nickel substrate by chemical vapor deposition:Wrin- kle formation.Adv Mater,2009,21:2328-2333
[109]
20 Wang X B,You H J,Liu F M,et al.Large-scale synthesis of few-layered graphene using CVD.Chem Vap Depos,2009,15:53-56
[110]
21 Kim K S,Zhao Y,Jang H,et al.Large-scale pattern growth of graphene films for stretchable transparent electrodes.Nature,2009,457:706-710
[111]
22 Li X S,Cai W W,An J H,et al.Large-area synthesis of high-quality and uniform graphene films on copper foils.Science,2009,324:1312-1314
[112]
23 Gao L B,Ren W C,Xu H L,et al.Repeated growth and bubbling transfer of graphene with millimetre-size single-crystal grains using platinum.Nat Commun,2012,3:699
[113]
24 Rollings E,Gweon G H,Zhou S Y,et al.Synthesis and characterization of atomically thin graphite films on a silicon carbide substrate.J Phys Chem Solids,2006,67:2172-2177
[114]
1 Novoselov K S, Geim A K, Morozov S V, et al.Electric field effect in atomically thin carbon films.Science, 2004, 306:666-669
[115]
2 Geim A K, Novoselov K S.The rise of graphene.Nat Mater, 2007, 6:183-191
[116]
3 Lee C, Wei X, Kysar J W, et al.Measurement of the elastic properties and intrinsic strength of monolayer graphene.Science, 2008, 321:385-388
[117]
4 Morozov S, Novoselov K, Katsnelson M, et al.Giant intrinsic carrier mobilities in graphene and its bilayer.Phys Rev Lett, 2008, 100:016602
[118]
5 Bolotin K I, Sikes K J, Jiang Z, et al.Ultrahigh electron mobility in suspended graphene.Solid State Commun, 2008, 146:351-355
[119]
6 Balandin A A, Ghosh S, Bao W, et al.Superior thermal conductivity of single-layer graphene.Nano Lett, 2008, 8:902-907
[120]
7 Park S, Ruoff R S.Chemical methods for the production of graphenes.Nat Nanotechnol, 2009, 4:217-224
[121]
8 Stoller M D, Park S, Zhu Y, et al.Graphene-based ultracapacitors.Nano Lett, 2008, 8:3498-3502
[122]
9 Nair R R, Blake P, Grigorenko A N, et al.Fine structure constant defines visual transparency of graphene.Science, 2008, 320:1308
[123]
10 Novoselov K S, Geim A K, Morozov S V, et al.Two-dimensional gas of massless dirac fermions in graphene.Nature, 2005, 438:197-200
[124]
11 Kim H, Abdala A A, Macosko C W.Graphene/polymer nanocomposites.Macromolecules, 2010, 43:6515-6530
[125]
12 Liu Y C, Dong X C, Chen P.Biological and chemical sensors based on graphene materials.Chem Soc Rev, 2012, 41:2283-2307
[126]
13 Bai H, Li C, Shi G Q.Functional composite materials based on chemically converted graphene.Adv Mater, 2011, 23:1089-1115
[127]
14 Huang X, Zeng Z Y, Fan Z X, et al.Graphene-based electrodes.Adv Mater, 2012, 24:5979-6004
[128]
25 Mathieu C,Barrett N,Rault J,et al.Microscopic correlation between chemical and electronic stat es in epitaxial graphene on SiC{0001}. Phys Rev B,2011,83:235436
[129]
26 Van Wesep R G,Chen H,Zhu W,et al.Communication:Stable carbon nanoarches in the initial stages of epitaxial growth of gra phene on Cu(111).J Chem Phys,2011,134:171105
[130]
27 Berger C,Song Z,Li X,et al.Electronic confinement and coherence in patterned epitaxial graphene.Science,2006,312:1191-1196
[131]
28 Emtsev K V,Speck F,Seyller T,et al.Interaction,growth,and ordering of epitaxial graphene on SiC{0001}surfaces:A compa rative photoelectron spectroscopy study.Phys Rev B,2008,77:155303
[132]
29 Yang X,Dou X,Rouhanipour A,et al.Two-dimensional graphene nanoribbons.J Am Chem Soc,2008,130:4216-4217
[133]
30 Carissan Y,Klopper W.Growing graphene sheets from reactions with methyl radicals:A qua ntum chemical study.Chem Phys Chem,2006,7:1770-1778
[134]
31 Qian H,Negri F,Wang C,et al.Fully conjugated tri(perylene bisimides):An approach to the construction of n-type graphene nanorib- bons.J Am Chem Soc,2008,130:17970-17976
[135]
32 Wang Z Y,Li N,Shi Z S,et al.Low-cost and large-scale synthesis of graphene nanosheets by arc discharge in air.Nanotechnology,2010,21:175602
[136]
33 Li N,Wang Z Y,Zhao K K,et al.Large scale synthesis of N-doped multi-layered graphene sheets by simple arc-discharge method.Car- bon,2010,48:255-259
[137]
34 Hirsch A.Unzipping carbon nanotubes:A peeling method for the formation of graphene nanoribbons.Angew Chem Int Ed,2009,48:6594-6596
[138]
35 Kosynkin D V,Higginbotham A L,Sinitskii A,et al.Longitudinal unzipping of carbon nanotubes to form graphene nanoribbons.Nature,2009,458:872-876
[139]
36 Zhang W X,Cui J C,Tao C A,et al.A strategy for producing pure single-layer graphene sheets based on a confined self-assembly ap- proach.Angew Chem Int Ed,2009,48:5864-5868
[140]
37 Kim C D,Min B K,Jung W S.Preparation of graphene sheets by the reduction of carbon monoxide.Carbon,2009,47:1610-1612
[141]
38 Meyer J C,Geim A K,Katsnelson M I,et al.The structure of suspended graphene sheets.Nature,2007,446:60-63
[142]
39 Becerril H A,Mao J,Liu Z,et al.Evaluation of solution-processed reduced graphene oxide films as transparent conductors.ACS Nano,2008,2:463-470
[143]
40 Shin H J,Kim K K,Benayad A,et al.Efficient reduction of graphite oxide by sodium borohydride and its effect on electrical conduct- ance.Adv Func Mater,2009,19:1987-1992
[144]
41 Cassagneau T,Fendler J H.Preparation and layer-by-layer self-assembly of silver nanoparticles capped by graphite oxide nanosheets.J Phys Chem B,1999,103:1789-1793
[145]
42 Stankovich S,Piner R D,Chen X,et al.Stable aqueous dispersions of graphitic nanoplatelets via the reduction of exfoliated graphite ox- ide in the presence of poly(sodium 4-styrenesulfonate).J Mater Chem,2006,16:155-158
[146]
43 Stankovich S,Dikin D A,Piner R D,et al.Synthesis of graphene-based nanosheets via chemical reduction of exfoliated graphite oxide. Carbon,2007,45:1558-1565
[147]
44 Fan X B,Peng W X,Li Y,et al.Deoxygenation of exfoliated graphite oxide under alkaline conditions:A green route to graphene prep a- ration.Adv Mater,2008,20:4490-4493
[148]
45 Li D,Müller M B,Gilje S,et al.Processable aqueous dispersions of graphene nanosheets.Nat Nanotechnol,2008,3:101-105
[149]
46 Zhu Y,Stoller M D,Cai W,et al.Exfoliation of graphite oxide in propylene carbonate and thermal reduction of the resulting graphene oxide platelets.ACS Nano,2010,4:1227-1233
[150]
47 Chen W F,Yan L F.Preparation of graphene by a low-temperature thermal reduction at atmosphere pressure.Nanoscale,2010,2:559-563
[151]
48 Dreyer D R,Murali S,Zhu Y,et al.Reduction of graphite oxide using alcohols.J Mater Chem,2011,21:3443-3447
[152]
49 Wei A,Wang J X,Long Q,et al.Synthesis of high-performance graphene nanosheets by thermal reduction of graphene oxide.Mater Res Bull,2011,46:2131-2134
[153]
50 Zhang H B,Wang J W,Yan Q,et al.Vacuum-assisted synthesis of graphene from thermal exfoliation and reduction of graphite oxide.J Mater Chem,2011,21:5392-5397
[154]
51 McAllister M J,Li J L,Adamson D H,et al.Single sheet functionalized graphene by oxidation and thermal expansion of graphi te.Chem Mater,2007,19:4396-4404
[155]
52 Chen W,Yan L,Bangal P R.Preparation of graphene by the rapid and mild thermal reduction of graphene oxide induced by micro waves. Carbon,2010,48:1146-1152
[156]
53 Schniepp H C,Li J L,McAllister M J,et al.Functionalized single graphene she ets derived from splitting graphite oxide.J Phys Chem B,2006,110:8535-8539
[157]
63 Lotya M,Hernandez Y,King P J,et al.Liquid phase production of graphene by exfoliation of graphite in surfactant/water sol utions.J Am Chem Soc,2009,131:3611-3620
[158]
64 O'Neill A,Khan U,Nirmalraj P N,et al.Graphene dispersion and exfoliation in low boiling point solvents.J Phys Chem C,20 11,115:5422-5428
[159]
65 Hernandez Y,Lotya M,Rickard D,et al.Measurement of multicomponent solubility parameters for graphene facilit ates solvent discov- ery.Langmuir,2010,26:3208-3213
[160]
66 Khan U,O'Neill A,Lotya M,et al.High-concentration solvent exfoliation of graphene.Small,2010,6:864-871
[161]
67 Khan U,O'Neill A,Porwal H,et al.Size selection of dispersed,exfoliated graphene flakes by controlled centrifugation.Carbon,2012,50:470-475
[162]
68 Keeley G P,O'Neill A,Holzinger M,et al.DMF-exfoliated graphene for electrochemical nadh detection.Phys Chem Chem Phys,2011,13:7747-7750
[163]
69 Hamilton C E,Lomeda J R,Sun Z,et al.High-yield organic dispersions of unfunctionalized graphene.Nano Lett,2009,9:3460-3462
[164]
70 Coleman J N.Liquid-phase exfoliation of nanotubes and graphene.Adv Func Mater,2009,19:3680-3695
[165]
71 Hummers W S,Offeman R E.Preparation of graphitic oxide.J Am Chem Soc,1958,80:1339-1339
[166]
15 Huang X, Yin Z, Wu S, et al.Graphene-based materials:Synthesis, characterization, properties, and applications.Small, 2011, 7:1876-1902
17 Sutter P W, Flege J I, Sutter E A.Epitaxial graphene on ruthenium.Nat Mater, 2008, 7:406-411
[169]
18 Reina A, Jia X, Ho J, et al.Large area, few-layer graphene films on arbitrary substrates by chemical vapor deposition.Nano Lett, 2008, 9:30-35
[170]
19 Chae S J, Güne? F, Kim K K, et al.Synthesis of large-area graphene layers on poly-nickel substrate by chemical vapor deposition:Wrinkle formation.Adv Mater, 2009, 21:2328-2333
[171]
20 Wang X B, You H J, Liu F M, et al.Large-scale synthesis of few-layered graphene using CVD.Chem Vap Depos, 2009, 15:53-56
[172]
21 Kim K S, Zhao Y, Jang H, et al.Large-scale pattern growth of graphene films for stretchable transparent electrodes.Nature, 2009, 457:706-710
[173]
22 Li X S, Cai W W, An J H, et al.Large-area synthesis of high-quality and uniform graphene films on copper foils.Science, 2009, 324:1312-1314
[174]
23 Gao L B, Ren W C, Xu H L, et al.Repeated growth and bubbling transfer of graphene with millimetre-size single-crystal grains using platinum.Nat Commun, 2012, 3:699
[175]
24 Rollings E, Gweon G H, Zhou S Y, et al.Synthesis and characterization of atomically thin graphite films on a silicon carbide substrate.J Phys Chem Solids, 2006, 67:2172-2177
[176]
25 Mathieu C, Barrett N, Rault J, et al.Microscopic correlation between chemical and electronic states in epitaxial graphene on SiC{0001}.Phys Rev B, 2011, 83:235436
[177]
26 Van Wesep R G, Chen H, Zhu W, et al.Communication:Stable carbon nanoarches in the initial stages of epitaxial growth of graphene on Cu(111).J Chem Phys, 2011, 134:171105
[178]
27 Berger C, Song Z, Li X, et al.Electronic confinement and coherence in patterned epitaxial graphene.Science, 2006, 312:1191-1196
[179]
28 Emtsev K V, Speck F, Seyller T, et al.Interaction, growth, and ordering of epitaxial graphene on SiC{0001} surfaces:A comparative photoelectron spectroscopy study.Phys Rev B, 2008, 77:155303
[180]
29 Yang X, Dou X, Rouhanipour A, et al.Two-dimensional graphene nanoribbons.J Am Chem Soc, 2008, 130:4216-4217
[181]
30 Carissan Y, Klopper W.Growing graphene sheets from reactions with methyl radicals:A quantum chemical study.Chem Phys Chem, 2006, 7:1770-1778
[182]
31 Qian H, Negri F, Wang C, et al.Fully conjugated tri(perylene bisimides):An approach to the construction of n-type graphene nanoribbons.J Am Chem Soc, 2008, 130:17970-17976
[183]
32 Wang Z Y, Li N, Shi Z S, et al.Low-cost and large-scale synthesis of graphene nanosheets by arc discharge in air.Nanotechnology, 2010, 21:175602
[184]
33 Li N, Wang Z Y, Zhao K K, et al.Large scale synthesis of N-doped multi-layered graphene sheets by simple arc-discharge method.Carbon, 2010, 48:255-259
[185]
34 Hirsch A.Unzipping carbon nanotubes:A peeling method for the formation of graphene nanoribbons.Angew Chem Int Ed, 2009, 48:6594-6596
[186]
35 Kosynkin D V, Higginbotham A L, Sinitskii A, et al.Longitudinal unzipping of carbon nanotubes to form graphene nanoribbons.Nature, 2009, 458:872-876
[187]
36 Zhang W X, Cui J C, Tao C A, et al.A strategy for producing pure single-layer graphene sheets based on a confined self-assembly approach.Angew Chem Int Ed, 2009, 48:5864-5868
[188]
37 Kim C D, Min B K, Jung W S.Preparation of graphene sheets by the reduction of carbon monoxide.Carbon, 2009, 47:1610-1612
[189]
38 Meyer J C, Geim A K, Katsnelson M I, et al.The structure of suspended graphene sheets.Nature, 2007, 446:60-63
[190]
39 Becerril H A, Mao J, Liu Z, et al.Evaluation of solution-processed reduced graphene oxide films as transparent conductors.ACS Nano, 2008, 2:463-470
[191]
40 Shin H J, Kim K K, Benayad A, et al.Efficient reduction of graphite oxide by sodium borohydride and its effect on electrical conductance.Adv Func Mater, 2009, 19:1987-1992
[192]
41 Cassagneau T, Fendler J H.Preparation and layer-by-layer self-assembly of silver nanoparticles capped by graphite oxide nanosheets.J Phys Chem B, 1999, 103:1789-1793
[193]
42 Stankovich S, Piner R D, Chen X, et al.Stable aqueous dispersions of graphitic nanoplatelets via the reduction of exfoliated graphite oxide in the presence of poly(sodium 4-styrenesulfonate).J Mater Chem, 2006, 16:155-158
[194]
43 Stankovich S, Dikin D A, Piner R D, et al.Synthesis of graphene-based nanosheets via chemical reduction of exfoliated graphite oxide.Carbon, 2007, 45:1558-1565
[195]
44 Fan X B, Peng W X, Li Y, et al.Deoxygenation of exfoliated graphite oxide under alkaline conditions:A green route to graphene preparation.Adv Mater, 2008, 20:4490-4493
[196]
45 Li D, Müller M B, Gilje S, et al.Processable aqueous dispersions of graphene nanosheets.Nat Nanotechnol, 2008, 3:101-105
[197]
46 Zhu Y, Stoller M D, Cai W, et al.Exfoliation of graphite oxide in propylene carbonate and thermal reduction of the resulting graphene oxide platelets.ACS Nano, 2010, 4:1227-1233
[198]
47 Chen W F, Yan L F.Preparation of graphene by a low-temperature thermal reduction at atmosphere pressure.Nanoscale, 2010, 2:559-563
[199]
48 Dreyer D R, Murali S, Zhu Y, et al.Reduction of graphite oxide using alcohols.J Mater Chem, 2011, 21:3443-3447
[200]
49 Wei A, Wang J X, Long Q, et al.Synthesis of high-performance graphene nanosheets by thermal reduction of graphene oxide.Mater Res Bull, 2011, 46:2131-2134
[201]
50 Zhang H B, Wang J W, Yan Q, et al.Vacuum-assisted synthesis of graphene from thermal exfoliation and reduction of graphite oxide.J Mater Chem, 2011, 21:5392-5397
[202]
51 McAllister M J, Li J L, Adamson D H, et al.Single sheet functionalized graphene by oxidation and thermal expansion of graphite.Chem Mater, 2007, 19:4396-4404
[203]
72 Brodie B C.On the atomic weight of graphite.Philos Trans R Soc london,1859,149:249-259
[204]
73 Staudenmaier L.Verfahren zur darstellung der graphitsaure.Ber Deut Chem Ges,1898,31:1481-1499
[205]
74 Dhakate S R,Chauhan N,Sharma S,et al.An approach to produce single and double layer graphene from re-exfoliation of expanded graphite.Carbon,2011,49:1946-1954